The output will not be what you want, because you're comparing two sets that will be completely different.
The first set will have a number of values for _time that correspond to the time periods the first search covers, which is from 3 days ago up until 2 days ago. The second set on the other hand will have times that include the last day up until now. So set diff will look at these sets, compare them and see that these are different on every line.
I'm not sure I follow what you want to do with timechart if all you want is two sets of IP's (also not sure what the eval command before that is for). If you tell us more about what you're trying to achieve it will be easier to help you. set diff would be one option, but this sounds like something that should be doable just using subsearches as well.
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